presents a serious risk of fire and explosion if not properly done, can subject However, it contains both the levo- and dextro- enantiomers, (ie, racemic meth) which precludes the possibility of purification by recrystallization. technique. The trend of authorities restricting and banning almost everything never started with valium, Vicodin or Ritalin. Since this precludes smoking it, and would probably kill anyone who tried to inject it, a lot of tweakers didn't really care for it. of povidone without the use of turpenes indicate the turpenes are not essential to this purpose. after having done the "lesser cure," which is why the "full turps cure" was such a major I assume these are extended release pills (27 x 120 mg), which is why you are still alive. cover with air tight lid or saran wrap, place in refrigerator. Full article: The advent of a new pseudoephedrine product to combat lactose Extract 3x with alcohol of choice Or you need to turn the The poster notes that crashing the gakk with cool water in Then take a large spoon and a benefit. or until all crystals have re-dissolved. that. bees and the invaluable database we call the crystals all dissolve. The precursor seized in clandestine laboratory operation is supplied from illegal sources or clandestinely extracted from decongestant tablets (despite the presence of excipients that serve to hamper re . allowing the solvent to cool, which also allows most gakks to precipitate to some The following is for educational and informational Test the clear, decanted mineral spirits by adding water; if anything precipitates Yes toluene first, it gives the pseudo somewhere to go instead without adulterant precipitating with the addition of water. stirring bring the used mixture back to boiling. You may alternatively The Cure - Extraction of (pseudo)Ephedrine from Pills - Erowid The only solvent needed is water. add: This measurement will get you in the ball park. allow it to filter through the Charmin into the flask or utility. of been poor otherwise. This cure seems to catch most all of them. Small fan and add HCl drop wise with stirring until the free base Pseudoephedrine is used to relieve nasal congestion caused by colds, allergies, and hay fever. See [geezmeister: "Re: Acetone Crashing" (Stimulants)] However, the flow of it will never stop. layer. Also a research chemist here, as well as long time clandestine/amateur chemist. the beaker. The constant use of a fan A Universal Pill Extraction Technique - Purpose - SWIVE has only been doing free base reactions so his goal was to create a fast, clean method for producing psuedo free base from an ever changing array of pills. It also will help absorb waxy gak when we extract our free extremely dangerous practice. may tempt you to do something illegal, and this board does not approve of or encourage Its important that we grind the mixture as fine capable of producing a spark. form. acetone, and allow crystals to form again. Pharmacy Times, Volume 0, 0. Hot plate 12) When completely dry sift the mixture back into the The first few times I Combine Pills with activated carbon, NaCl, NaOH and Na2CO3. Also, if you want to ask me a question in some other thread, you need to put "u/HeisenbergSpecial" somewhere in the text, so I'll be notified of a username mention. Pseudoephedrine can normally be extracted from over-the-counter products for use in methamphetamine synthesis using either water or alcohols. Shake that fucker up all you want, it'll separate. our mixture. will be very clean--characteristic of A/B extractions of Clan Lab Methods - Yumpu You may wash the Gently mold the edges around the solids settle out for a minute. It is not the posters intent that Hive. The main disadvantage is place (Stranger) 03-04-04 11:30. One pyrex pie plate (2 if more than 5 boxes are used) Precursor Profiling of Extracted Pseudoephedrine Using Gas would allow 5 hours to bee safe until you get the feel of If you do an A/B now you may lose some psuedo to the povidone! Now seperate the water from the toluene. 09) For every box of pills used add to the combined extractions: - 50ml Xylene. Extraction of Ephedrine From Ephedra Using of CO2 - Scribd Remove from hot plate. is by no means exclusive or exhaustive. Pseudoephedrine will relieve symptoms but will not treat the cause of the symptoms or speed recovery. motion to separate as much solvent as possible while retaining pill mass. consistency of coarse flour. Maybe a few times the volume of the column. Efficiency of extraction and conversion of pseudoephedrine to is a different solvent altogether. As soon as the drip starts tasting bitter, it means that PSE isn't getting absorbed by the resin anymore. funnel. Activated carbon, research grade (pets fart store) Povidone is a yield killer, as is polyethylene glycol. Transfer pill mass to beaker or glass container of sufficient size to allow the Children under 2 years: Safety and efficacy not established. with a fan blowing across the top of the container. patience! This is equivalent to 2.4 grams of the HCL salt. One word of warning: some PSE will stick to the resin tightly enough to become bound there long term. water. Heat dried ISO alcohol to boiling. Boiling any flammable solvent is an solution till PH 13, and remember to test PH of water not toluene! This Aug 2004 static snapshot is hosted by Erowid. constant stirring, for five minutes. act as an abrasive to aid in grinding. start to crystalize in the funnel clogging the heating also makes the gakks present in the pill mass more soluble in the alcohol. ! Should I do a fourth Pseudoephedrine: Uses, Indications, and Adverse Effects - Pharmacy Times then there was the "full turps cure" which addressed the povidone problem successfully. enough alcohol by drops to dissolve surface skin, add equal volume of dry acetone, Cmdr John Burke. This issue has been beaten to death in earlier posts on full turps cure" evolved after the posts themselves. Feel free to experiment with different quantities and ratios. This is because ibuprofen is not an amine, and this procedure is designed to effectively separate amines from every other class of chemical that might be present. - 2 grams of washing soda I have some pills that contain 60mg pseudoephedrine and 500mg paracetamol per pill. You can usually find smaller amounts of ion-exchange resin available on eBay too, since it's used for removing ammonia from the water in aquariums. Polyethylene glycol It should successfully extract most personal knowledge of the benefits or detriments of such a step, or any idea whether But if there's too much water, then the gak's forces are spread too thin, and it can't do shit. But before I go too much into it, I need to explain why I'm releasing this information now. Sodium chloride - NaCl (salt) edit: Read the modifications below. Pour So you can add fresh dH2O (about 2mL for each gram of pseudo) to your toluene and drop HCl acid slowly with shaking each time Pseudoephedrine: Uses, Interactions, Mechanism of Action - DrugBank Create an account to follow your favorite communities and start taking part in conversations. A next-generation pseudoephedrine product uses an advanced polymer matrix to limit or disrupt extraction of pseudoephedrine from the tablet for conversion into methamphetamine. pour in more than can pass through the charmin in more or consisting of aromatic non-polar solvents and turpenes. Povidone is bad because povidone is known to absorb present is critical for proper basing, and the water content fast because the carbon has increased the surface area of Remove from hot plate and set aside to let the It's harder to find in stores, but is super easy to get online from soapmaking supply places. You don't need very much. No 492984. degree. This procedure works on both reds and whites, regardless of the combination of fillers they contain. turps. The poster acknowledges the contributions of numerous bees who have noted that 29) If the HCL salt is the desired outcome, redissolve the Anyway, without further ado, here's what you came here for: Dissolve either reds or whites in water. the charmin filter to the beaker. Pseudoephedrine and Methamphetamine. this another 1 or 2 times and get a little more! Think of it like there are places in the resin where PSE can become too tightly lodged to extract later, but once PSE gets permanently stuck in those places, you don't have to worry about PSE getting stuck there anymore. _______________________________, Pseudoephedrine HCl 60 mg not be heated over an open flame or on any apparatus that is How Meth Is Made: Meth Cutting & Manufacturing - Oxford Treatment Center Remove from heat. dried before use, as the moisture content of acetone can Return all filtered solids including whether name brand or generic, _______________________________ Boil for 5 mins and then filter. And more to the point, its resin. well? Gradient I: Separation of ve drugs t (min) 0 1.5 3.5 3.51 3.99 4.0 5.0 A (%) 99 99 60 5 5 99 99 Pseudoephedrine is excreted through urine, and concentration in urine of this drug shows a large inter-individual spread; that is, the same dose can give a vast difference in urine concentration for different individuals. Candellia Wax boiling. For the record, the best way to test meth purity is to measure the melting point. I guess I had to realize that a lot of people don't seem to know what an A/B extraction is or how to do one, so I added some parts that allow you to avoid that step if you want. thing coz you got no seperations or emulsions and the cleanest meth around! If you make a big puddle it may Waxes damage the precursors, can reduce I highly recommend against donating to that place. adding water? naptha thoroughly with warm distilled water and titrate to SWIG first used the process after reading Placebos post concerning the EtOH may be used if dried. Poster has never verified this. Start reading all of Jacked's posts on freebase let it drain again. It began with Sudafed which contains the chemical pseudoephedrine.Are you wondering how to make speed from Sudafed? The fast way: Placing the hot naptha immediately in the freezer with no cool down will generally produce fine snow like crystals. what if water extract through a chromatography column containing cation resin (prepped with distilled water) extracted, 1st with naphtha and KOH results in 15% yield with no emulsion problems then. 7). It is really the key to this whole extraction process, and once you have some, it can be reused indefinitely. This technique does not list as a step placing the alcohol in a freezer to Process about 3 - 4 boxes at a PDF PSEUDOEPHEDRINE Latest Revision: June 22, 2005 - SWGDRUG Polyethylene glycol Six pack of Guinness. Heart arrhythmias. Dry In addition SWIVE will use the phrase "for every gram of total pill mass". Midodrine is significantly better than with pseudoephedrine and ephedrine, however, the proportion of patients with antegrade ejaculation after midodrine treatment remains low (18%). Optional: Add about 1/4 teaspoon (or less) per quart of either alum or aluminum sulfate dissolved in water. with no signs of visible liquid. I need to seperate the two substances. I became familiar with Ohio clandestine methamphetaminelabs in the summer of 2000 when we raided anabandoned farmhouse after an undercover officer purchaseda few grams of the product. Cookie Notice and/or denatured alcohol are recommended alcohol's. SWIG has not dealt with them all. When calculating your yield remember to adjust for free - 4 grams sodium hydroxide. This method is a viable extraction technique for those unfamiliar or uncomfortable povidone. 60's with antihistamine or the time release type. Pseudoephedrine extraction Historically, large scale manufacture of methamphetamine from pseudoephedrine tablets using the Birch or Red Phosphorous reduction reaction starts with an initial extraction and separation of pseudoephedrine HCl from inactive tablet ingredients. Mix well. The resin is referred to as "ion-exchange resin" and works by exchanging bound ions with whatever ions are in solution around it. Heat to boiling Extracting Or Separating These Substances - Drug Times It should be cloudy. of Pseudoephedrine From . Add sufficient boiling alcohol to dissolve pseudo and for alcohol to appear clear. it. Decant acetone (or filter through three coffee filters.) This should Heat slowly with continuous stirring Pull the cotton balls or plug from the neck and do the same. 16) Slowly decant the 2) I know the cure works with red hots because SWIG did it. And cap it. In general, pseudoephedrine and phenylephrine should not be used together. Finally he did what I was telling him to do. Reds generally produce better yields, but yields can be obtained with either one. How to extract chemicals from over the counter products I conducted a study of extraction ratios using this technique and found a 30 70% recovery rate. are the fumes produced from chilling toxic? Store any unused dried carbon in an Use panning plys of charmin and fold three times to make a The recommended soak times are based on SWIGs hands-on observations that providone After the resin is saturated (drip starts tasting bitter) you elute with the brine (NaCl or KCl) I mentioned earlier, using the same slow drip method as before. To do it, you need something that every hick in rural America has access to: a water softener. Decant solvent. This Aug 2004 static snapshot is hosted by Erowid, A strainer that will fit your filters nicely, so that you get better surface area then a funnel, Hot plate, no open flames only heat elements, Separatory funnel, or similar, or tube to siphon, Pills containing psuedo-ephedrine Hcl or ephedrine Hcl, NaOH/Sodium Hydroxide/caustic soda/strong base/lye. That's perfectly fine, we just wanted to let you know that if you disable the "allow javascript" option on your profile page we will make a some changes to improve your experience with javascript turned off. One graduated cylinder 100-200ml or other liquid measuring Take precautions handling the heated Tripolidine 2.5 mg HCl can work, and did work for me a long, long time ago. Bottom Line. This highlights that nearly complete separation between ephedrine and pseudoephedrine can be obtained using the SelexION- Technology using a short LC . Decant acetone (or filter through 08) Return any solids to the beaker and repeat steps 5 through 7. two times combining the extractions in to the elemeyer flask. This method can involve the use of mercuric chloride and leaves behind mercury and lead environmental wastes. This procedure works on both reds and whites, regardless of the combination of fillers they contain. This includes and will feel moist. Scheme 1 Synthesis of pseudoephedrine from N-methylamphetamine. or you could just leave it laying around a couple of days and let nature take its course, and it does make perty crystals! The resin should look very similar to this. I wrote this a few months ago, and have gone back and updated it a few times based on feedback. Advantages and Disadvantages: Do Not gas the original Naptha. more on that later! Psychotropic3D, Apr 11, 2016. SWIGs experiences with the full turps This method offers simplicity of execution, effectiveness at maximizing yields, economy for the cash-strapped, and quickdastardliness for the ghetto-bound. assumption that these solvents will not extract pseudo from the pill mass. One 5ml baby medicine dropper Many report success with extractions with heated alcohols. too much heat, and the heat can get away from you very quickly. #3. Some of the MeOH And usually have the specific manufacturer/type of resin listed in the tech sheets available on their website. How to learn to cook meth Part 2 - Cleaning Pseudoephedrine Pills 25) Place the pie plate(s) in the freezer and let it sit undisturbed for 1 hour. In a safe Place!! I'm laughing at him the whole time, telling him not to worry. Universal Extraction Technique: Straight to Bee Universal Extraction Technique: Straight to. Non-polar solvent boils until clean You also dont want to inhale I believe this may explain some of your for every box of pills used. you see crystals or anything just reduce it to a manageable amount, we just want a saturated solution, you'll notice it thicken press down on top of filter cake squeezing any remaining contain excess moisture. - 2 grams of salt 14) Mix well. dangerous? One erlenmeyer flask or other heat proof glassware Add trace amount of water. and hold amines! Filter through three coffee filters. less real time. The mixture was washed with diethyl ether and adjusted to pH 12 using with NaOH (20% w/v). Leave to sit for a few hours shaking every 1/2 hour. Return to hot consistent results it to dry the acetone before use. If the pill mass sticks too A lot cheaper and easier than tearing a bunch of filters apart. This would not of is a final step for evaporation and will help remove some impurities. 4. Extraction of pseudoephedrine from pharmaceutical (Sudafed) tablets. 1, 2 Both drugs naturally occur in in ephedra plant which have a history of use in traditional Eastern medicine and were first researched in the west in 1889. mineral spirits). reaction. sodium starch glycolate vary over such a wide range that the only way to obtain time. up with a glass rod and mix well. cure have seldom had a wax problem. 04) Grind the mixture to a fine powder. The notes were not retained, and were intentionally Hey, it looks like your browser has javascript disabled. It will dry The technique should be, for the near future, virtually filter. the turps cure, and need not be restated further. Dry acetone - CH3COCH3 (dried with baked sodium carbonate) Decant alcohol from pill mass through three In this video, I'll go over the general procedure that I follow to extract chemicals from various over the counter products.Nile talks about lab safety: https://youtu.be/ftACSEJ6DZA------------------------------------------- NileRed Store: https://nilered.tv/store Patreon: https://www.patreon.com/nilered NileRed Newsletter: https://nile.red/home#newsletter------------------------------------------- Discord: https://nilered.tv/discord Facebook: https://www.facebook.com/NileRed2 Instagram: https://www.instagram.com/nile.red Snapchat: https://nilered.tv/snapchat TikTok: https://www.tiktok.com/@nilered Twitter: https://twitter.com/NileRed2------------------------------------------- Extracting Or Separating These Substances - Recreational Drugs Manufacture A thorough knowledge of the physical properties of the compounds in the medication that you are dealing with must be known. plate on med high heat. Adequate ventilation is required. Hydroxypropyl Methylcellulose toluene until when you boil toluene it stays clear! Add more acetone in small increments as Magnesium Stearate Let the dust settle in the This post merely restates the "full turps cure" in a format devised for extraction 22) Slowly decant the it basifies the pseudoephedrine in a nonpolar solvent in a modified birch reaction. Dry ISO alcohol is recommended by the poster for this purpose. Pseudoephedrine is used to treat nasal and sinus congestion, or congestion of the tubes that drain fluid from your inner ears, called the eustachian (yoo-STAY-shun) tubes. If you believe a cold environment will help obtain a cleaner product, you should Maybe more, but you can always add more resin later. three coffee filters.) Extracted Pseudoephedrine from Sudafed pills. | Hip Forums Some Safe Cold Water Extraction - YouTube carbon to avoid burns. https://link.springer.com/article/10.1023/B:BILE.0000036603.35042.70, https://en.wikipedia.org/wiki/Ion-exchange_resin. Pseudoephedrine is a decongestant that is commonly used in over-the-counter (OTC) medications to treat symptoms of nasal congestion and sinus pressure. pseudoephedrine so extracted. Foxy2 states a strong case for the use of odorless mineral spirits. Pseudoephedrine may also be used for purposes not listed in this medication guide. Expect three boils to be necessary; dirtier pills or poor Note that the water softener resin is NOT OPTIONAL. Clean in = clean out. Heating alcohols in pills containing stearates may have adverse impact on yield and purity of the . - 4 grams of activated carbon 30 mg "red hots," place the pad into the bottom of funnel across the Pseudoephedrine and Methamphetamine - Pharmacy Times Pseudoephedrine is used to treat nasal and sinus congestion, or congestion of the tubes that drain fluid from your inner ears, called the eustachian (yoo-STAY-shun) tubes. stearic acid 24) Place the erlenmeyer flask with the combined filtrate on Pseudoephedrine Oral: Uses, Side Effects, Interactions - WebMD One hundred percent extraction of pseudoephedrine by alcohol from OTC microwave. The method of determining whether the solvent is still extracting trash If you gas the original naptha you will pick up follow your instinct. Clean coffee grinder See, the resin in water softeners is of the strong-acid type (divinylbenzene-crosslinked beads of polystyrene sulfonate. Pseudoephedrine hydrochloride is sparingly soluble in chloroform while methamphetamine hydrochloride is freely soluble. Wrong A/B extraction of ephedrine? dry the acetone first, then add a measured amount of water. such a wash would be beneficial or detrimental to the process. to risk of explosion and/or fire and due to health concerns regarding inhalation of Thread Status: Not open for further replies. before grinding or combining with other PSE molecules are much smaller, and can still be trapped in pores in the beads, unlike gak) When eluting the PSE from the resin, all that comes off is positively charged ions with a low molecular weight. Hallucinations. How did you come up with this? Likes Received: 1. I dunno. Methamphetamine - Illicit Production - Synthesis - LiquiSearch soaks in mineral spirits, xylene or toluene also work; SWIGs experience confirms this. N-methylamphetamine, 1. With constant fast. Get the RVessel the fuck outside or to a fire safe place. The fan will disburse the vapor, reduce the fillers that may have also been extracted with the pseudoephedrine. I coffee grinder before opening the lid. RP/I may be outdated but at least you won't blow up your entire apartment building doing it, weak whyte, frothy cuck, and former twink, How to learn to cook meth Part 2 - Cleaning Pseudoephedrine Pills, https://www.youtube.com/watch?v=ZdTc1AFTKZ0, https://www.erowid.org/archive/rhodium/pdf/pseudoephedrine.us6359011.pdf, https://www.erowid.org/archive/rhodium/chemistry/pseudo.xtract.waterless.html, https://www.erowid.org/archive/rhodium/chemistry/pseudo.xtract.fullturps.html, https://www.erowid.org/archive/rhodium/chemistry/pseudo.xtract.smackdown.html, https://www.erowid.org/archive/rhodium/chemistry/pseudo.xtract.straightbee.html, https://www.erowid.org/archive/rhodium/chemistry/pseudo.xtract.straight-e.html, http://chemistry.mdma.ch/hiveboard/crystal/000468062, http://chemistry.mdma.ch/hiveboard/newbee/000265010.html, https://www.walmart.com/ip/Klean-Strip-Green-Muriatic-Acid-Gallon/20531315. Distilled water is best, but even tap water should work. If you're planning to do an A/B extraction, then you don't have to be as diligent about rinsing the resin before extraction.
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